Sangam: A Confluence of Knowledge Streams

Expanding the Dimensions of a Small, Two-Dimensional Diffraction Detector

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dc.contributor Massachusetts Institute of Technology. Department of Materials Science and Engineering
dc.creator Chen, Xi
dc.creator Hauwiller, Matthew R
dc.creator Kumar, Abinash
dc.creator Lebeau, James M
dc.date 2020-09-30T13:59:38Z
dc.date 2020-09-30T13:59:38Z
dc.date 2020-08
dc.date 2020-09-30T12:11:21Z
dc.date.accessioned 2023-03-01T18:08:50Z
dc.date.available 2023-03-01T18:08:50Z
dc.identifier 1431-9276
dc.identifier https://hdl.handle.net/1721.1/127774
dc.identifier Chen, Xi et al. “Expanding the Dimensions of a Small, Two-Dimensional Diffraction Detector.” Microscopy and Microanalysis, 11, (August 2020): 1-6 © 2020 The Author(s)
dc.identifier.uri http://localhost:8080/xmlui/handle/CUHPOERS/278925
dc.description We report an approach to expand the effective number of pixels available to small, two-dimensional electron detectors. To do so, we acquire subsections of a diffraction pattern that are then accurately stitched together in post-processing. Using an electron microscopy pixel array detector (EMPAD) that has only 128 × 128 pixels, we show that the field of view can be expanded while achieving high reciprocal-space sampling. Further, we highlight the need to properly account for the detector position (rotation) and the non-orthonormal diffraction shift axes to achieve an accurate reconstruction. Applying the method, we provide examples of spot and convergent beam diffraction patterns acquired with a pixelated detector.
dc.description United States. Air Force. Office of Scientific Research (Grant FA9550-17-1-0225)
dc.description National Science Foundation (U.S.) (Award ECCS-1542015)
dc.description National Science Foundation (U.S.) (Grant DMR-1726294)
dc.format application/pdf
dc.language en
dc.publisher Cambridge University Press (CUP)
dc.relation 10.1017/s1431927620024277
dc.relation Microscopy and Microanalysis
dc.rights Creative Commons Attribution-Noncommercial-Share Alike
dc.rights http://creativecommons.org/licenses/by-nc-sa/4.0/
dc.source Prof. LeBeau via Ye Li
dc.title Expanding the Dimensions of a Small, Two-Dimensional Diffraction Detector
dc.type Article
dc.type http://purl.org/eprint/type/JournalArticle


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